Each test method shall include or reference the following, where applicable:
- (1) Identification of the test method;
- (2) Applicable matrix or matrices;
- (3) Detection limit;
- (4) Scope and application, including components to be analyzed;
- (5) Summary of the test method;
- (6) Definitions;
- (7) Interferences;
- (8) Safety;
- (9) Equipment and supplies;
- (10) Reagents and standards;
- (11) Sample collection, preservation, shipment and storage;
- (12) Quality control;
- (13) Calibration and standardization;
- (14) Procedure;
- (15) Calculations;
- (16) Method performance;
- (17) Pollution prevention;
- (18) Data assessment and acceptance criteria for quality control measures;
- (19) Corrective actions for out-of-control data;
- (20) Contingencies for handling out-of-control or unacceptable data;
- (21) Waste management;
- (22) References; and
- (23) Any tables, diagrams, flowcharts and validation data.
Added at 25 Ok Reg 2247, eff 7-11-08