Ariz. Admin. Code § R9-14-621 – Time-frames

A. The overall time-frame described in A.R.S. § 41-1072 for each type of approval granted by the Department under this Article is set forth in Table 6.1.
1. 1. An applicant and the Department may agree in writing to extend the substantive review time-frame and the overall time-frame.
2. 2. An extension of the substantive review time-frame and the overall time-frame may not exceed 25% of the overall time-frame.
B. The administrative completeness review time-frame described in A.R.S. § 41-1072 for each type of approval granted by the Department under this Article is set forth in Table 6.1 and begins on the date that the Department receives an application or request for approval.
1. 1. The Department shall send a notice of administrative completeness or deficiencies to an applicant within the administrative completeness review time-frame.
  1. a. A notice of deficiencies shall list each deficiency and the information or items needed to complete the application or request for approval.
  2. b. The administrative completeness review time-frame and the overall time-frame are suspended from the date that a notice of deficiencies is sent until the date that the Department receives all of the missing information or items from an applicant.
2. 2. If an applicant fails to submit to the Department all of the information and items listed in a notice of deficiencies within 60 days after the date that the Department sent the notice of deficiencies, the Department shall consider the application or request for approval withdrawn.
3. 3. If the Department issues a license or other approval to an applicant during the administrative completeness review time-frame, the Department shall not issue a separate written notice of administrative completeness.
C. The substantive review time-frame described in A.R.S. § 41-1072 is set forth in Table 6.1 and begins on the date of a notice of administrative completeness.
1. 1. As part of the substantive review for an initial license application, the Department may conduct a laboratory inspection, investigation, or proficiency testing, or a combination of the three, as described in R9-14-605.
  1. a. The Department shall commence a laboratory inspection, investigation, or proficiency testing, or combination of the three, no more than 30 days after notice of administrative completeness has been mailed for an in-state laboratory or no more than 60 days after notice of administrative completeness has been mailed for an out-of-state laboratory.
  2. b. The Department and an applicant may mutually agree in writing to schedule a laboratory inspection, proficiency testing, or investigation later than the date required under subsection (C)(1)(a).
2. 2. The Department shall send written notification of approval or denial of a license or other approval to an applicant within the substantive review time-frame.
3. 3. During the substantive review time-frame, the Department may make one comprehensive written request for additional information, unless the Department and applicant have agreed in writing to allow the Department to submit supplemental requests for information.
4. 4. If the Department issues a comprehensive written request or a supplemental request for information, the substantive review time-frame and the overall time-frame are suspended from the date that the Department issues the request until the date that the Department receives all of the information requested.
5. 5. If an applicant fails to submit to the Department all of the information and items listed in a comprehensive written request or a supplemental request for information within 60 days after the date that the Department sent the comprehensive written request or supplemental request for information, the Department shall deny the license or other approval requested.
6. 6. The Department shall grant a license or other approval unless:
  1. a. An applicant fails to submit requested information or a requested item as described in subsection (B)(2) or (C)(5);
  2. b. For an initial license application or a regular license renewal application where the regular license is not suspended, the Department determines that grounds to deny the license exist under A.R.S. § 36-495.09;
  3. c. For a regular license renewal application where the regular license is suspended, the Department determines that the licensee is not in full compliance with the corrective action plan; A.R.S. Title 36, Chapter 4.3; or this Article;
  4. d. For a request for approval of an alternate method or method alteration, the Department determines that the alternate method or method alteration does not meet the standard for approval under R9-14-610(E); or
  5. e. For a request for approval of an exemption under R9-14-615(D), the Department determines that the request does not meet the standard for approval under R9-14-615(F).
7. 7. If the Department denies a license or other approval, the Department shall send to the applicant a written notice of denial setting forth the reasons for denial and all other information required by A.R.S. § 41-1076.

Table 6.1. Time-frames (in days)

Type of Approval	Statutory Authority	Overall Time-frame	Administrative Completeness Review Time-frame	Substantive Review Time-frame
Initial License–In-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07	201	21	180
Initial License–Out-of-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07	231	21	210
Regular License Renewal–In-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07	37	14	23
Regular License Renewal–Out-of-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07, 36-495.14	67	14	53
Regular License Renewal–In-State Laboratory with Provisional License	A.R.S. §§ 36-495.01, 36-495.03, 36-495.05, 36-495.06, 36-495.07	70	21	49
Regular License Renewal–Out-of-State Laboratory with Provisional License	A.R.S. §§ 36-495.01, 36-495.03, 36-495.05, 36-495.06, 36-495.07, 36-495.14	100	21	79
Request for Approval of an Alternate Method or Method Alteration–Required or Authorized by EPA/ADEQ	A.R.S. §§ 36-495.01, 36-495.06	105	15	90
Request for Approval of an Alternate Method or Method Alteration–Due to an Approved Method Not Being Available	A.R.S. §§ 36-495.01, 36-495.06	210	30	180
Request for Approval of an Exemption under R9-14-615(D)	A.R.S. § 36-495.01	60	15	45
Request to Have One or More Parameters Added to a License under R9-14-620 – In-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07	91	21	70
Request to Have One or More Parameters Added to a License under R9-14-620 –Out-of-State Laboratory	A.R.S. §§ 36-495.01, 36-495.03, 36-495.06, 36-495.07	121	21	100

Historical Note

New Table adopted by final rulemaking at 7 A.A.R. 184, effective December 15, 2000 (Supp. 00-4). Amended by final rulemaking at 12 A.A.R. 4798, effective December 5, 2006 (Supp. 06-4). Table 1 renumbered to Table 6.1 and amended by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Exhibit I. Repealed

Table 1. Repealed

Table 2. Repealed

Historical Note

Exhibit I made by final rulemaking at 12 A.A.R. 4798, effective December 5, 2006 (Supp. 06-4). Exhibit I, consisting of Tables 1 and 2, repealed by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Exhibit II. Repealed

Table 1. Repealed

Historical Note

Exhibit II made by final rulemaking at 12 A.A.R. 4798, effective December 5, 2006 (Supp. 06-4). Exhibit II, consisting of Table 1, repealed by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.2.A. Approved Methods and Method Fees for Drinking Water Parameters

1. Microbiology of Drinking Water
Description	Reference	Method/s	Fee Per Method
Aeromonas	A4.35	1605	$228
Coliforms, Fecal	C	9221E (2006)	$228
		9222D (2006)	$228
Coliforms, Total and E. coli, by Colilert (ONPG-MUG)	C and Z	9223B (2004) and IDEXX	$152
Coliforms, Total, and E. coli, by Colisure	C2 and Z7	9223B (2004) and IDEXX	$152
Coliforms, Total, by Membrane Filtration	C	9222B (2006)	$228
		9222C (2006)	$228
Coliforms, Total and E. coli, by Membrane Filtration	A4.36	1604	$228
Coliforms, Total, and E. coli by Colitag	C and Z5	9223B (2004) and CPI	$152
Coliforms, Total, and E. coli by Modified Colitag	C and D8	9223B (2004) and Modified Colitag	$152
Coliforms, Total, and E. coli by E.colite	C and Z8	9223B (2004) and Charm Sciences, Inc.	$152
Coliforms, Total, and E. coli by m-ColiBlue24 Test	C and Z6	9222H (2006) and Hach 10029	$228
Coliforms, Total, and E. coli by Readycult Coliforms 100 Presence/Absence	C and Z14	9223B (2004) and EM Science	$152
Coliforms, Total, and E. coli by MF using Chromocult Coliform Agar	C and Z15	9223B (2004) and EM Science	$152
Coliforms, Total, by Multiple Tube Fermentation	C	9221B and C (2006)	$228
Coliforms, Total, by Presence/Absence	C	9221D (2006)	$228
Escherichia coli	C	9222G (2006)	$228
	X	Tube Procedure	$228
		Membrane Filter Procedure	$228
Cryptosporidium	A4.32	1622	$381
Giardia and Cryptosporidium	A4.39	1623	$381
	A4.33	1623.1	$381
Heterotrophic Plate Count	C	9215B (2004)	$152
	Z3	SimPlate	$152
Heterotrophic Plate Count (For Bottled Water Only)	C	9215D (2004)	$152
Microscopic Particulate Analysis	P1	910/9-92-029	$228
Viruses	P2	600/R-95/178	$381
Coliphage	A4.37	1601	$228
	A4.38	1602	$228
2. Inorganic Chemistry and Physical Properties of Drinking Water
Description	Reference	Method/s	Fee Per Method
Alkalinity	C	2320B (2011)	$19
Asbestos	A4.30	100.1 (9/83)	$503
	A4.31	100.2 (6/94)	$503
Bromate	A4.1	317.0 (2.0)	$76
	A4.3	326.0 (1.0)	$76
	A5	300.1 (1.0)	$26
		321.8 (1.0)	$152
	A4.41	302.0 (1.0)	$26
Bromide	A2	300.0 (2.1)	$26
	A4.1	317.0 (2.0)	$76
	A4.3	326.0 (1.0)	$76
	A5	300.1 (1.0)	$26
Calcium	A1	200.7 (4.4)	$10
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3500-Ca B (2011)	$76
Carbon, Dissolved Organic	A4.12	415.3 (1.1)	$76
	A4.13	415.3 (1.2)	$76
	C	5310B (2011)	$39
		5310C (2011)	$39
		5310D (2011)	$39
Carbon, Total Organic	A4.12	415.3 (1.1)	$76
	A4.13	415.3 (1.2)	$76
	C	5310B (2011)	$39
		5310C (2011)	$39
		5310D (2011)	$39
Chloride	A2	300.0 (2.1)	$26
	A5	300.1 (1.0)	$26
	C	4500-Cl B (2011)	$39
		4500-Cl D (2011)	$39
		4110B (2011)	$26
Chloramine	C	4500-Cl F (2011)	$39
		4500-Cl G (2011)	$76
Chlorate	A5	300.1 (1.0)	$26
Chlorine, Total Residual and Free	A4.44	334.0 (9/2000)	$39
	C	4500-Cl D (2011)	$39
		4500-Cl E (2011)	$39
		4500-Cl F (2011)	$39
		4500-Cl G (2011)	$39
		4500-Cl H (2011)	$39
		4500-Cl I (2011)	$39
Chlorine Dioxide	A4.4	327.0 (1.1)	$76
	C	4500-ClO2 E (2011)	$39
	C7	ChlordioX Plus	$79
Chlorite	A2	300.0 (2.1)	$26
	A4.1	317.0 (2.0)	$76
	A4.3	326.0 (1.0)	$76
	A4.4	327.0 (1.1)	$76
	A5	300.1 (1.0)	$26
	C	4500-ClO2 E (2011)	$39
	C7	ChlordioX Plus	$79
Color	C	2120B (2011)	$32
Corrosivity	C	2330B (2010)	$39
Cyanide	A2	335.4 (1.0)	$76
	A6	QuikChem 10-204-00-1-X (2.1)	$76
	C	4500-CN B (2011)	$7
		4500-CN C (2011)	$13
		4500-CN E (2011)	$76
		4500-CN F (2011)	$76
	E7	Kelada-01	$76
Cyanide, Available/Amenable	A4.26	OIA-1677 DW	$76
	C	4500-CN G (2011)	$76
	I	D6888-04	$76
Fluoride	A2	300.0 (2.1)	$26
	A3	380-75WE (2/76)	$39
	A5	300.1 (1.0)	$26
	C	4500-F B (2011)	$39
		4500-F C (2011)	$26
		4500-F D (2011)	$39
		4500-F E (2011)	$39
		4110B (2011)	$26
Hardness	A1	200.7 (4.4), Sum of Ca and Mg as their carbonates	$10
	C	2340 B (2011), Sum of Ca and Mg as their carbonates	$10
		2340 C (2011)	$39
Magnesium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3500-Mg B (1997)	$76
Methylene Blue Active Substances	C	5540 C (2011)	$39
Nitrate	A2	300.0 (2.1)	$26
		353.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-NO3 D (2011)	$39
		4500-NO3 E (2011)	$76
		4500-NO3 F (2011)	$76
		4110B (2011)	$26
Nitrite	A2	300.0 (2.1)	$26
		353.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-NO2 B (2011)	$76
		4500-NO3 E (2011)	$76
		4500-NO3 F (2011)	$76
		4110B (2011)	$26
Odor	C	2150B (2011)	$32
Orthophosphate	A2	300.0 (2.1)	$26
		365.1 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-P E (2011)	$76
		4500-P F (2011)	$76
		4110B (2011)	$26
Ozone	C	4500-O3 B (2011)	$39
Perchlorate	A4.2	314.1 (1.0)	$76
	A4.5	331.0 (1.0)	$76
	A4.11	332.0 (1.0)	$76
	A5	314.0 (1.0)	$76
pH (Hydrogen Ion)	A	150.1	$39
		150.2	$39
	C	4500-H B (2011)	$39
Residue, Filterable (TDS)	C	2540C (2011)	$39
Sediment Concentration	I	D 3977-97	$13
Silica	A1	200.7 (4.4)	$10
	A4.10	200.5 (4.2)	$10
	C	4500-SiO2 C (2011)	$76
		4500-SiO2 D (2011)	$76
		4500-SiO2 E (2011)	$76
Sodium	A1	200.7 (4.4)	$10
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
Specific Conductance	C	2510B (2011)	$39
Sulfate	A2	300.0 (2.1)	$26
		375.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-SO4 C (2011)	$76
		4500-SO4 D (2011)	$76
		4500-SO4 E (2011)	$76
		4500-SO4 F (2011)	$76
		4110B (2011)	$26
Temperature, Degrees Celsius	C	2550 (2010)	$13
Turbidity, Nephelometric (NTU)	A2	180.1 (2.0)	$39
	C	2130B (2011)	$39
UV-Absorption at 254 nm	A4.12	415.3 (1.1)	$76
	A4.13	415.3 (1.2)	$76
	C	5910B (2011)	$76
3. Metals in Drinking Water
a. Sample Preparation for Metals in Drinking Water
Description	Reference	Method/s	Fee Per Method
Acid Extractable Metals	C	3030C (2004)	$7
Microwave Assisted Digestion	C	3030K (2004)	$7
Nitric Acid	C	3030E (2004)	$7
Nitric Acid/Hydrochloric Acid	C	3030F (2004)	$7
Nitric Acid/Perchloric Acid	C	3030H (2004)	$7
Nitric Acid/Perchloric Acid/Hydrofluoric Acid	C	3030I (2004)	$7
Nitric Acid/Sulfuric Acid	C	3030G (2004)	$7
Preliminary Filtration	C	3030B (2004)	$7
b. Methods to Analyze Metals in Drinking Water
Description	Reference	Method/s	Fee Per Method
Aluminum	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3113B (2010)	$26
Antimony	A1	200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
Arsenic	A1	200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
		3114B (2011)	$76
Barium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3113B (2010)	$26
Beryllium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
Cadmium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
Chromium, Hexavalent by IC	A4.43	218.7 (1.0)	$116
Chromium, Total	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
Cobalt	A1	200.8 (5.4)	$26
Copper	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
Iron	A1	200.7 (4.4)	$10
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
Lead	A1	200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
Manganese	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	C	3111B (2011)	$26
		3113B (2010)	$26
Mercury	A	245.2	$52
	A1	245.1 (3.0)	$52
		200.8 (5.4)	$26
	C	3112B (2011)	$52
Molybdenum	A1	200.8 (5.4)	$26
Nickel	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
Selenium	A1	200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
		3114B (2011)	$76
Silver	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
Strontium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	C	3500-Sr B (2011)	$26
		3500-Sr C (2011)	$20
		3500-Sr D (2011)	$26
Thallium	A1	200.8 (5.4)	$26
		200.9 (2.2)	$26
Uranium	A1	200.8 (5.4)	$26
	C	7500 U-C (2011)	$206
	I	D3972-97, 02	$206
		D5174-97, 02	$206
Vanadium	A1	200.8 (5.4)	$26
Zinc	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
4. Organic Chemistry of Drinking Water
a. Methods to Comply with National Primary Drinking Water Regulations
Description	Reference	Method/s	Fee Per Method

Disinfectant Byproducts, Solvents and Pesticides:

Alachlor

Atrazine

Dibromochloropropane

Endrin

Ethylene dibromide

Heptachlor

Heptachlorepoxide

Hexachlorobenzene

Hexachlorocyclopentadiene

Lindane

Methoxychlor

Simazine

1,1,2-Trichloroethane

Trichloroethylene

1,1,1-Trichloroethane

Tetrachloroethylene

Carbontetrachloride

Chloroform

Bromodichloromethane

Dibromochloromethane

Bromoform

Total Trihalomethanes

551.1 (1.0)

$116

VOCs by GC:

Benzene

Carbon Tetrachloride

(mono) Chlorobenzene

o-Dichlorobenzene

para-Dichlorobenzene

1,2-Dichloroethane

cis-1,2-Dichloroethylene

Trans-1,2-Dichloroethylene

Dichloromethane

1,2-Dichloropropane

Ethylbenzene

Styrene

Tetrachloroethylene

1,1,1-Trichlorothane

Trichloroethylene

Toluene

1,2,4-Trichlorobenzene

1,1-Dichloroethylene

1,1,2-Trichloroethane

Vinyl chloride

Xylenes, Total

Chloroform

Bromodichloromethane

Dibromochloromethane

Bromoform

Total Trihalomethanes

502.2 (2.1)

$152

VOCs by GC-MS:

Benzene

Carbon Tetrachloride

(mono) Chlorobenzene

o-Dichlorobenzene

para-Dichlorobenzene

1,2-Dichloroethane

cis-1,2-Dichloroethylene

Trans-1,2-Dichloroethylene

Dichloromethane

1,2-Dichloropropane

Ethylbenzene

Styrene

Tetrachloroethylene

1,1,1-Trichlorothane

Trichloroethylene

Toluene

1,2,4-Trichlorobenzene

1,1 Dichloroethylene

1,1,2-Trichloroethane

Vinyl Chloride

Xylenes, Total

Chloroform

Bromodichloromethane

Dibromochloromethane

Bromoform

Total Trihalomethanes

	A4.19	524.4	$152
	D3	524.2 (4.1)	$152

VOCs by GC:

Benzene

Carbon Tetrachloride

(mono) Chlorobenzene

o-Dichlorobenzene

para-Dichlorobenzene

1,2-Dichloroethane

cis-1,2-Dichloroethylene

Trans-1,2-Dichloroethylene

Dichloromethane

1,2-Dichloropropane

Ethylbenzene

Styrene

Tetrachloroethylene

1,1,1-Trichlorothane

Trichloroethylene

Toluene

1,2,4-Trichlorobenzene

1,1-Dichloroethylene

1,1,2-Trichloroethane

Vinyl chloride

Xylenes, Total

Chloroform

Bromodichloromethane

Dibromochloromethane

Bromoform

Total Trihalomethanes

Dibromochloropropane

Ethylenedibromide	A4.20	524.3 (1.0)	$152
EDB/DBCP	D3	504.1 (1.1)	$116

Pesticides and PCBs by GC (Microextraction):

Alachlor

Atrazine

Chlorodane

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorocyclopentadiene

Lindane

Methoxychlor

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Simazine

Toxaphene

505 (2.1)

$152

Phthalate and Adipate Esters by GC-PID:

Di (2-ethylhexyl)adipate

Di (2-ethylhexyl)phthalate

506 (1.1)

$116

Pesticides by GC-NPD

Atrazine

Alachlor

Simazine

507 (2.1)

$116

Chlorinated Pesticides by GC-ECD:

Chlordane

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorocyclopentadiene

Lindane

Methoxychlor

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Toxaphene

508 (3.1)

$152

Chlorinated Pesticides, Herbicides,

Organohalides by GC-ECD:

Alachlor

Atrazine

Chlorodane

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorocyclopentadiene

Lindane

Methoxychlor

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Simazine

Toxaphene

508.1(2.0)

$152

Organics by GC-MS:

Alachlor

Atrazine

Benzo(a)pyrene

Chlorodane

Di (2-ethylhexyl)adipate

Di (2-ethylhexyl)phthalate

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorocyclopentadiene

Lindane

Methoxychlor

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Pentachlorophenol

Simazine

Toxaphene	D3	525.2 (2.0)	$152
1, 4-Dioxane by GC/MS	A4.21	522	$152

Carbamates by HPLC/Post Column:

Carbofuran

Oxamyl	A4.8	531.2 (1.0)	$116
	D3	531.1 (3.1)	$116

Chlorinated Acids and Dalapon by GC-ECD:

2,4-D

Dalapon

Dinoseb

Pentachlorophenol

Picloram

Silvex (2,4,5-TP)	A4.6	515.4 (1.0)	$116
	A5	515.3 (1.0)	$116
	D	515.1 (4.0)	$116

Chlorinated Acids By GC-ECD

2,4-D

Dinoseb

Pentachlorophenol

Picloram

Silvex (2,4,5-TP)

515.2 (1.1)

$116

Haloacetic Acids, Bromate and Dalapon

By IC-ESI-MS/MS	A4.18	557 (1.0)	$152
Perfluorinated Compounds by LC/MS/MS	A4.40	537 (1.1)	$152
Hormones by LC/MS/MS	A4.42	539	$152

PAHs By HPLC/UV/FL:

Benzo(a)pyrene	D1	550 (7/90)	$116
		550.1 (7/90)	$116

Haloacetic Acids and Dalapon by GC-ECD:

Dalapon

Monochloracetic Acid

Dichloracetic Acid

Trichloroacetic Acid

Monobromoacetic Acid

Dibromoacetic Acid

HAA5	D2	552.1 (1.0)	$116
	D3	552.2 (1.0)	$116

Haloacetic Acids:

Monochloroacetic Acid

Dichloroacetic Acid

Trichloroacetic Acid

Monobromoacetic Acid

Dibromoacetic Acid

Dalapon

HAA5	A4.9	552.3 (1.0)	$116
Disinfection Byproducts by Micro Liquid-Liquid Extraction/GC-ECD	C8	6251B (1994)	$116

Chlorinated Acids By HPLC/PDA/UV:

2,4-D

Dinoseb

Pentachlorophenol

Picloram

Silvex (2,4,5-TP)	D2	555 (1.0)	$116
1,4 Dioxane by GC/MS	A4.21	522 (1.0)	$152
Dioxin	A4.22	1613 Rev B (10/94)	$258
Diquat	A5	549.2 (1.0)	$116
Endothall	D2	548.1 (1.0)	$116
Glyphosate	D1	547 (7/90)	$116
PCBs (as decachlorobiphenyl)	D	508A (1.0)	$152
b. Additional Methods and Compounds Required by Other Programs
Description	Reference	Method/s	Fee Per Method
Disinfectant Byproducts, Solvents and Pesticides	D3	551.1 (1.0)	$26
VOCs by GC	D3	502.2 (2.1)	$26
VOCs by GC-MS	A4.20	524.3 (1.0)	$26
	D3	524.2 (4.1)	$26
EDB/DBCP	D3	504.1 (1.1)	$26
Pesticides and PCBs by GC (Microextraction)	D3	505 (2.1)	$26
Phthalate and Adipate Esters by GC-PID	D3	506 (1.1)	$26
Pesticides by GC-NPD	D3	507 (2.1)	$26
Chlorinated Pesticides by GC-ECD	D3	508 (3.1)	$26
Chlorinated Pesticides, Herbicides, Organohalides by GC-ECD	D3	508.1(2.0)	$26
Organics by GC-MS	D3	525.2 (2.0)	$26
Carbamates by HPLC/Post Column	A4.8	531.2 (1.0)	$26
	D3	531.1 (3.1)	$26
Chlorinated Acids and Dalapon by GC-ECD	A4.6	515.4 (1.0)	$26
	A5	515.3 (1.0)	$26
	D	515.1 (4.0)	$26
Chlorinated Acids By GC-ECD	D3	515.2 (1.1)	$26
PAHs By HPLC/UV/FL	D1	550 (7/90)	$26
		550.1 (7/90)	$26
Haloacetic Acids and Dalapon by GC-ECD	D2	552.1 (1.0)	$26
	D3	552.2 (1.0)	$26
Chlorinated Acids By HPLC/PDA/UV	D2	555 (1.0)	$26
Dioxins and Furans	A4.22	1613 Rev B (10/94)	$65
Paraquat	A5	549.2 (1.0)	$26
Benzidines and Nitrogen Compounds	D2	553 (1.1)	$116
Carbonyl Compounds	D2	554 (1.0)	$116
Phenols	A5	528 (1.0)	$152
Phenylurea Compounds	A5	532 (1.0)	$116
Selected Semivolatiles	A5	526 (1.0)	$152
Pesticides and Flame Retardants by GCMS	A4.7	527 (1.0)	$152
Explosives and Related Compounds	A4.15	529 (1.0)	$152
Acetanilide Degradation Products	A4.16	535 (1.1)	$194
Acetanilide Parent Compound	D3	525.2 (2.0)	$26
Nitrosamines by MS/MS	A4.14	521 (1.0)	$194
5. Radiochemistry of Drinking Water
Description	Reference	Method/s	Fee Per Method
Cesium	B	p. 4	$206
	C	7500-Cs B (2011)	$206
		7120 (2011)	$206
	J	R-1110-76	$206
		R-1111-76	$206
	L	901	$206
		901.1	$206
	U	Ga-01-R	$206
	W	p. 92	$206
Gamma Emitters	C	7500-Cs B (2011)	$206
		7500-I B (2011)	$206
		7120 (2011)	$206
	L	901.1	$206
		901.0	$206
		902.0	$206
	U	Ga-01-R	$206
	W	p. 92	$206
Gross Alpha	B	EPA 00-02	$206
	C	7110C (2011)	$206
	L	900.0	$206
	V	00-01	$206
		00-02	$206
Gross Alpha and Beta	B	p. 1	$206
	C	7110B (2011)	$206
	J	R-1120-76	$206
	L	900.0	$206
	V	00-01	$206
	W	p. 1	$206
Iodine	B	p. 6, p. 9	$206
	C	7120 (2011)	$206
		7500-I B (2011)	$206
		7500-I C (2011)	$206
		7500-I D (2011)	$206
	L	901.1	$206
		902.0	$206
	U	Ga-01-R	$206
	W	p. 92	$206
Radium 226	B	p. 13, p. 16	$206
	C	7500-Ra B (2011)	$206
		7500-Ra C (2011)	$206
	L	903.0	$206
		903.1	$206
	U	Ra-04	$206
		Ra-05	$206
	V	EPA Ra-03	$206
		EPA Ra-04	$206
	W	p. 19	$206
Radium 228	B	p. 24	$206
	C	7500-Ra D (2011)	$206
	L	904.0	$206
	V	Ra-05	$206
	W	p. 19	$206
Strontium	B	p. 29	$206
	C	7500-Sr B (2011)	$206
	J	R-1160-76	$206
	L	905.0	$206
	U	Sr-01	$206
		Sr-02	$206
	V	Sr-04	$206
	W	p. 65	$206
Tritium	B	p. 34	$206
	C	7500-3H B (2011)	$206
	J	R-1171-76	$206
	L	906.0	$206
	V	H-02	$206
	W	p.87	$206
Uranium	A1	200.8 (5.4)	$26
	A7	D5174-97, 02	$206
	C	7500-U B (2011)	$206
		7500-U C (2011)	$206
	J	R-1180-76	$206
		R-1181-76	$206
		R-1182-76	$206
	L	908.0	$206
		908.1	$206
	U	U-02	$206
		U-04	$206
	V	00-07	$206
	W	p. 33	$206

Historical Note

New Table 6.2.A. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.2.B. Approved Methods and Method Fees for Wastewater Parameters

1. Microbiology of Wastewater and Sewage Sludge
Description	Reference	Method/s	Fee Per Method
Ascaris lumbricoides	C8	10550	$228
	P3	UofA2000	$228
Coliforms, Fecal, number per 100 ml or number per gram dry weight, by Membrane Filter	C	9222D (2006)	$228
Coliforms, Fecal, by Multiple Tube Fermentation (may be used for sewage sludge), number per 100 ml by MPN	C	9221C, E (2006)	$228
Coliforms, Total, by Membrane Filter	C	9222B (2006)	$228
Coliforms, Total, by Multiple Tube Fermentation	C	9221B (2006)	$228
Control of pathogens and vectors in sewage	E3	625/R-92/013	$76
Cryptosporidium	A4.32	1622	$381
Cryptosporidium and Giardia	A4.39	1623	$381
	C	9711B (2011)	$381
	P2	600/R-95/178	$381
E. coli, number per 100 ml, MPN multiple tube	C	9222B (2006)	$228
E. coli, number per 100 ml, MPN multiple tube/multiple well	C	9223B (2004)	$228
E. coli by m-ColiBlue	C1 and Z6	Hach 10029	$228
Enterococci, number per 100 ml MF	C	9230C (2007)	$228
Escherichia coli by Colilert MPN, in conjunction with SM 9221B and 9221C	C	9223B (2004)	$152
Escherichia coli in conjunction with SM 9221B and 9221C	C	9221F (2006)	$152
Entamoeba histolytica	C	9711C (2011)	$228
Enteric viruses	I	D4994-89	$381
Enteric viruses in sewage sludge	E3	EPA 625/R-92/103	$381
Fecal Coliforms by Colilert-18 (APP and Reuse only)	C	9020B (2005)/9223B (2004)	$152
Fecal Coliforms by Colilert-18 (NPDES-ATP Permits only)	C	9020B (2005)/9223B (2004)	$152
Fecal Coliforms in sewage sludge by MTF	Z1	EPA 1681	$228
Helminth Ova in sludge	Z4	600/1-87-014	$381
Salmonella in sludge MPN	E5	9260D (1988)	$228
Salmonella in Sewage Sludge (Biosolids) by Modified MSRV	A4.34	1682	$228
Streptococcus, Fecal, by Membrane Filter	C	9230C (2007)	$194
Streptococcus, Fecal, by Multiple Tube Fermentation	C	9230B (2007)	$194
Viruses	C	9510 (2011)	$381
	P	Methods for Virology	$381
	P2	600/R-95/178	$381
2. Wastewater Inorganic Chemistry, Nutrients and Demand
Description	Reference	Method/s	Fee Per Method
Acid Mine Drainage	A4.27	1627	$303
Acidity	C	2310B (2011)	$39
Alkalinity, Total	A	310.2 (1974)	$19
	C	2320B (2011)	$19
Ammonia	A2	350.1 (2.0)	$39
	C	4500-NH3 B (2011)	$39
		4500-NH3 C (2011)	$39
		4500-NH3 D (2011)	$39
		4500-NH3 E (2011)	$39
		4500-NH3 G (2011)	$39
	C1	Hach 10205	$39
Ammonia in sludge only	E5	4500-NH3B&C (1990)	$39
Biochemical Oxygen Demand/Carbonaceous Biochemical Oxygen Demand	C	5210B (2011)	$152
	C3	Hach 10360	$152
Boron	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	4500-B B (2011)	$76
Bromide	A2	300.0 (2.1)	$26
	A5	300.1 (1.0)	$26
Calcium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3500-Ca B (2011)	$39
Carbon, Total Organic (TOC)	C	5310 B (2011)	$39
		5310 C (2011)	$39
		5310D (2011)	$39
Chemical Oxygen Demand	A	410.3 (1978)	$39
	A2	410.4 (2.0)	$76
	C	5220 B (2011)	$39
		5220 C (2011)	$39
		5220 D (2011)	$76
	C1	Hach 8000	$39
Chloride	A2	300.0 (2.1)	$26
	A5	300.1 (1.0)	$26
	C	4500-Cl B (2011)	$39
		4500-Cl C (2011)	$39
		4500-Cl D (2011)	$39
		4500-Cl E (2011)	$39
Chlorine, Total Residual	C	4500-Cl B (2011)	$39
		4500-Cl C (2011)	$39
		4500-Cl D (2011)	$39
		4500-Cl E (2011)	$39
		4500-Cl F (2011)	$39
		4500-Cl G (2011)	$39
	C1	Hach 10014	$39
Color	C	2120 B (2011)	$32
Cyanide, Available	C	4500-CN G (2011)	$76
	E7	Kelada-01	$76
	Y	OIA-1677-09 (8/99)	$76
Cyanide, Free	Y	OIA-1677-09 (8/99)	$76
Cyanide, Total	A2	335.4 (1.0)	$76
	A6	QuickChem 10-204-00-1-X (2.1)	$76
	C	Combination of 4500-CN B (2011) and 4500-CN C (2011), followed by 4500-CN D (2011), 4500-CN E (2011), or 4500-CN F (2011)	$89
	E7	Kelada-01	$76
Fluoride	A2	300.0 (2.1)	$26
	A5	300.1 (1.0)	$26
	C	4500-F B (2011)	$39
		4500-F C (2011)	$39
		4500-F D (2011)	$39
		4500-F E (2011)	$39
Hardness	A	130.1 (1976)	$10
	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	2340B (2011)	$39
		2340C (2011)	$39
Kjeldahl, Total Nitrogen	A	351.1 (1978)	$76
	A2	351.2 (2.0)	$76
	C	Combination of 4500-NH3 B (2011) and either 4500-Norg B (2011) or 4500-Norg C (2011)	$115
		4500-NH3 C (2011)	$39
		4500-NH3 D (2011)	$39
		4500-NH3 E (2011)	$39
		4500-NH3 F (2011)	$39
		4500-NH3 G (2011)	$39
		4500-NH3 H (2011)	$39
	Z9	PAI-DK01 (12/94)	$76
	Z10	PAI-DK02 (12/94)	$76
	Z11	PAI-DK03 (12/94)	$76
Methylene Blue Active Substances	C	5540C (2011)	$39
Nitrate (as N)	A	352.1 (1971)	$76
	A2	300.0 (2.1)	$26
	A5	300.1 (1.0)	$26
	C	3500-NO3 D (2011)	$39
Nitrate-Nitrite (as N)	A2	300.0 (2.1)	$26
		353.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-NO3 E (2011)	$76
		4500-NO3 F (2011)	$76
		4500-NO3 H (2011)	$76
Nitrite (as N)	A2	300.0 (2.1)	$26
		353.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-NO2 B (2011)	$76
		4500-NO3 E (2011)	$76
		4500-NO3 F (2011)	$76
Oil and Grease and Total Petroleum Hydrocarbons	A4.24	1664 Rev B	$76
	C	5520B (2011)	$76
Orthophosphate	A	365.3 (2.0)	$76
	A2	300.0 (2.1)	$26
		365.1 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-P E (2011)	$76
		4500-P F (2011)	$76
Oxygen-consumption Rate (SOUR)	C	2710B (2011)	$39
Oxygen, Dissolved	C	4500-O B (2011)	$26
		4500-O C (2011)	$26
		4500-O D (2011)	$26
		4500-O E (2011)	$26
		4500-O F (2011)	$26
		4500-O G (2011)	$26
	C1	1002-8-2009	$26
	C3	Hach 10360	$26
pH (Hydrogen Ion)	A	150.2	$39
	C	4500-H B (2011)	$39
Phenols	A	420.1 (1978)	$116
	A2	420.4 (1.0)	$116
	C	5530 B (2010)	$116
		5530 D (2010)	$116
Phosphorus, Total	A	365.3 (1978)	$76
		365.4 (1974)	$76
	A1	200.7 (4.4)	$10
	A2	365.1 (2.0)	$76
	C	4500-P B (2011)	$76
		4500-P E (2011)	$76
		4500-P F (2011)	$76
		4500-P G (2011)	$76
		4500-P H (2011)	$76
Potassium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	C	3111B (2011)	$26
		3500-K B (2011)	$26
Residue, Filterable (TDS)	C	2540C (2011)	$39
	E8	I-1750-85	$39
Residue, Nonfilterable (TSS)	C	2540D (2011)	$39
Residue, Settleable Solids	C	2540F (2011)	$39
Residue, Total	C	2540B (2011)	$39
Residue, Volatile	A	160.4 (1971)	$39
	C	2540E (2011)	$39
Silica, Dissolved	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	4500-SiO2 B (2011)	$76
		4500-SiO2 C (2011)	$76
		4500-SiO2 E (2011)	$76
		4500-SiO2 F (2011)	$76
Sodium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3500-Na B (2011)	$26
		3500-Na D (2011)	$26
		3111B (2011)	$26
Sodium Azide	C	4110C (2011)	$76
Specific Conductance	A	120.1 (1982)	$39
	C	2510B (2011)	$39
Sulfate	A2	300.0 (2.1)	$26
		375.2 (2.0)	$76
	A5	300.1 (1.0)	$26
	C	4500-SO4 C (2011)	$76
		4500-SO4 D (2011)	$76
		4500-SO4 E (2011)	$76
		4500-SO4 F (2011)	$76
		4500-SO4 G (2011)	$76
Sulfide (includes total and soluble)	C	4500-S2- B (2011)	$39
		4500-S2- D (2011)	$76
		4500-S2- F (2011)	$39
		4500-S2- G (2011)	$39
	C1	Hach 8131	$39
Sulfite	C	4500-SO3 B (2011)	$76
Temperature, Degrees Celsius	C	2550B (2010)	$13
Total, Fixed and Volatile Solids in Solid and Semisolid Samples in Sludge	C	2540G (2011)	$39
Turbidity, NTU	A2	180.1 (2.0)	$39
	C	2130B (2011)	$39
3. Metals in Wastewater
a. Sample Preparation for Metals in Wastewater
Description	Reference	Method/s	Fee Per Method
Acid Extractable Metals	C	3030C (2004)	$7
Digestion for Metals	C	3030D (2004)	$7
Microwave Digestion	E6	CEM Microwave Digestion	$7
Nitric Acid	C	3030E (2004)	$7
Nitric Acid/Hydrochloric Acid	C	3030F (2004)	$7
Nitric Acid/Perchloric Acid	C	3030H (2004)	$7
Nitric Acid/Perchloric Acid/Hydrofluoric Acid	C	3030I (2004)	$7
Nitric Acid/Sulfuric Acid	C	3030G (2004)	$7
Preliminary Filtration	C	3030B (2004)	$7
b. Methods to Analyze Metals in Wastewater
Description	Reference	Method/s	Fee Per Method
Aluminum	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
		3111D (2011)	$26
Antimony	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3113B (2010)	$26
Arsenic	A	206.5 (1978)	$39
	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
		3500-As B (2011)	$76
Barium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3113B (2010)	$26
Beryllium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3111E (2011)	$26
		3113B (2010)	$26
Cadmium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
		3500-Cd D (2011)	$76
Chromium (VI) Hexavalent	A1	218.6 (3.3)	$26
	C	3500-Cr B (2011)	$39
		3111C (2011)	$26
Chromium, Total	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
		3500-Cr B (2011)	$76
Cobalt	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
Copper	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
		3500-Cu B (2011)	$76
		3500-Cu C (2011)	$76
Gold	A	231.2 (1978)	$26
	A1	200.8 (5.4)	$26
	C	3111B (2011)	$26
Iridium	A	235.2 (1978)	$26
	C	3111B (2011)	$26
Iron	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
		3500-Fe B (2011)	$76
Lead	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
		3500-Pb B (2011)	$76
Lithium	A1	200.7 (4.4)	$10
Magnesium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
Manganese	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
		3500-Mn B (2011)	$76
Mercury	A	245.2 (1974)	$52
	A1	200.7 (4.4)	$10
		245.1 (3.0)	$52
	A4.17	1631E	$152
	A4.23	245.7 (2.0)	$15
	C	3112B (2011)	$52
Molybdenum	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3113B (2010)	$26
Nickel	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
Osmium	A	252.2 (1978)	$26
	C	3111D (2011)	$26
Palladium	A	253.2 (1978)	$26
	C	3111B (2011)	$26
Platinum	A	255.2 (1978)	$26
	C	3111B (2011)	$26
Rhodium	A	265.2 (1978)	$26
	C	3111B (2011)	$26
Ruthenium	A	267.2 (1978)	$26
	C	3111B (2011)	$26
Selenium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3113B (2010)	$26
		3114B (2011)	$76
Silver	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3111C (2011)	$26
		3113B (2010)	$26
Strontium	A1	200.7 (4.4)	$10
	C	3111B (2011)	$26
		3500-Sr B (2011)	$26
		3500-Sr C (2011)	$20
		3500-Sr D (2011)	$26
Thallium	A	279.2 (1978)	$26
	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
Tin	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
		200.9 (2.2)	$26
	A4.10	200.5 (4.2)	$10
	C	3111B (2011)	$26
		3113B (2010)	$26
Titanium	A	283.2 (1978)	$26
	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	C	3111D (2011)	$26
Vanadium	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	C	3111D (2011)	$26
		3500-V B (2011)	$76
Zinc	A	289.2 (1978)	$26
	A1	200.7 (4.4)	$10
		200.8 (5.4)	$26
	A4.10	200.5 (4.2)	$10
	A4.25	1638	$26
	C	3111B (2011)	$26
		3111C (2011)	$26
		3500 Zn B (2011)	$76
4. Aquatic Toxicity Bioassay of Wastewater
Description	Reference	Method/s	Fee Per Method
Toxicity, Acute	M1	EPA/600/4-90/027F	$194
	Z12	821-R-02-012	$194
Toxicity, Chronic	N1	EPA/600/4-91/002	$194
	Z2	821-R-02-013	$194
	Z13	Lozarchak, J. 2001	$194
5. Organic Chemicals of Wastewater
Description	Reference	Method/s	Fee Per Method
Volatile Organics for Pharmaceuticals	D3	524.2 (4.1)	$152
Purgeable Hydrocarbons	E	601	$76
Purgeable Aromatics	E	602	$76
Acrolein and Acrylonitrile	E	603	$76
		624	$152
Phenols	E	604	$116
Benzidines	E	605	$116
Phthalate ester	E	606	$116
Nitrosamines	E	607	$116
Organochlorine Pesticides and PCBs	E	608	$152
	E2	608.1	$152
		608.2	$152
	E4	608 (3M)	$152
Nitroaromatics and Isophorone	E	609	$116
PAHs	E	610	$116
Haloethers	E	611	$116
Chlorinated Hydrocarbons	E	612	$116
2, 3, 7, 8-Tetrachlorodibenzo-p-Dioxin	E	613	$457
Chlorinated Herbicides	E2	615	$116
Organohalide Pesticides and PCB	E2	617	$116
Triazine Pesticides	E2	619	$116
Thiophosphate Pesticides	E2	622.1	$116
Purgeables	E	624	$152
Base/Neutrals and Acids (all analytes excluding pesticides)	E	625	$152
Base/Neutrals and Acids (pesticides only)	E	625	$152
Carbamate and Urea Compounds	E2	632	$116
Tetra- through Octa-Chlorinated Dioxins and Furans	A4.22	1613 Rev B (10/94)	$258
VOCs by Isotope Dilution GC/MS	E	1624B	$152
Semivolatile Organic Compounds by Isotope Dilution GC/MS	E	1625B	$152
Organophosphorus Pesticides	E1	1657	$116
	E2	614	$116
		614.1	$116
		622	$116
VOCs Specific to the Pharmaceutical Manufacturing Industry by Isotope Dilution GC/MS	K1	1666 (A)	$152
Herbicides	C	6640B (2006)	$116
Ethylene Glycol	K	BLS-188	$152
6. Radiochemistry of Wastewater
Description	Reference	Method/s	Fee Per Method
Alpha-Total pCi per liter	C	7110B (2011)	$206
	L	900.0	$206
Alpha Counting Error, pCi per liter	C	7110B (2011)	$206
Beta-Total pCi per liter	C	7110B (2011)	$206
	L	900.0	$206
Beta Counting Error, pCi	C	7110B (2011)	$206
Radium, Total pCi per liter	C	7500-Ra B (2011)	$206
	L	903.0	$206
Radium	C	7500-Ra C (2011)	$206
	L	903.1	$206

Historical Note

New Table 6.2.B. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.2.C. Approved Methods and Method Fees for Waste Parameters

1. Microbiology of Waste
Description	Reference	Method/s	Fee Per Method
Coliforms, Total, by Membrane Filter	F	9132	$228
Coliforms, Total, by Multiple Tube Fermentation	F	9131	$228
2. Sample Preparation for Waste
Description	Reference	Method/s	Fee Per Method
Acid Digestion of Water	F	3005A	$7
Alkaline Digestion for Hex Chome	F	3060A	$7
Bomb Preparation Method for Solid Waste	F	5050	$7
EP for Oily Wastes	F	1330A	$76
EP Toxicity	F	1310B	$76
Microwave Assisted Digestions	F	3015A	$7
		3051A	$7
		3052	$7
		3546	$7
Multiple EP	F	1320	$152
Oils, Greases, and Waxes	F	3040A	$7
Oils	F	3031	$7
Sediments, Sludges, and Soils	F	3050B	$7
SPLP	F	1312	$303
TCLP	F	1311	$303
Total Metals	F	3010A	$7
		3020A	$7
Total Recoverable in Water	F	3005A	$7
3. Inorganic Chemistry and Metals of Solid Waste
Description	Reference	Method/s	Fee Per Method
Aluminum	F	6010C	$10
		6020A	$26
		7000B	$26
	F and F13	6010D	$10
		6020B	$26
Ammonia	A	350.3	$39
Antimony	F	6010C	$10
		6020A	$26
		7062	$76
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Arsenic	F	6010C	$10
		6020A	$26
		7010	$26
		7061A	$76
		7062	$76
		7063	$76
	F and F13	6010D	$10
		6020B	$26
Barium	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Beryllium	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Boron	F	6010C	$10
	F and F13	6010D	$10
Bromide	F	9056A	$26
		9211	$39
Cadmium	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Calcium	F	6010C	$10
		6020A	$26
		7000B	$26
	F and F13	6010D	$10
		6020B	$26
Cation-Exchange Capacity of Soils	F	9080	$34
		9081	$34
Chloride	F	9056A	$26
		9057	$76
		9212	$39
		9250	$76
		9251	$76
		9253	$39
Chlorine, Total, in New and Used Petroleum Products	F	9075	$76
		9076	$39
		9077	$39
Chromium, Hexavalent	F	7195	$26
		7196A	$76
		7197	$26
		7198	$40
		7199	$76
Chromium, Total	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Cobalt	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Compatibility Test for Wastes and Membrane Liners	F	9090A	$152
Copper	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Corrosive to Steel	F	1110A	$63
Corrosivity pH Determination	F	9040C	$63
Cyanide	F	9010C	$13
		9012B	$76
		9213	$76
		9014	$76
	F9	9015	$76
Cyanide Extraction for Solids and Oils	F10	9013A	$39
Dermal Corrosion	F	1120	$63
Ignitability of Solids	F	1030	$32
Flash Point by Pensky Martems Cup	F	1010A	$32
Flash Point by Set-a Flash	F	1020B	$32
Fluoride	F	9056A	$26
		9214	$39
Iron	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Kjeldahl Total, Nitrogen	A	351.4	$76
Lead	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Liquid Release Test Procedure	F	9096	$39
Lithium	F	6010C	$10
		7000B	$26
	F and F13	6010D	$10
Magnesium	F	6010C	$10
		6020A	$26
		7000B	$26
	F and F13	6010D	$10
		6020B	$26
Manganese	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Mercury	F	6010C	$10
		6020A	$26
		7470A	$52
		7471B	$52
		7472	$152
		7473	$152
		7474	$152
	F and F13	6010D	$10
		6020B	$26
Molybdenum	F	6010C	$10
		7000B	$26
		7010	$26
	F and F13	6010D	$10
Nickel	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Nitrate	F	9210A	$39
		9056A	$26
Nitrite	F	9056A	$26
		9216	$39
Oil and Grease and Petroleum Hydrocarbons	A4.24	1664B	$76
O-Phosphate-P	F	9056A	$26
Osmium	F	7000B	$26
Paint Filter Liquids Test	F	9095B	$19
Perchlorate	A5	314.0	$76
	F	6850	$152
pH (Hydrogen Ion)	F	9041A	$39
		9045D	$39
Phosphorus	F	6010C	$10
	F and F13	6010D	$10
Phosphorus, Total	A	365.3	$76
Potassium	F	6010C	$10
		6020A	$26
		7000B	$26
	F and F13	6010D	$10
		6020B	$26
Saturated Hydraulic and Leachate Conductivity and Intrinsic Permeability	F	9100	$152
Selenium	F	6010C	$10
		6020A	$26
		7010	$26
		7741A	$26
		7742	$76
	F and F13	6010D	$10
		6020B	$26
Silica	F	6010C	$10
	F and F13	6010D	$10
Silver	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Sodium	F	6010C	$10
		6020A	$26
		7000B	$26
	F and F13	6010D	$10
		6020B	$26
Sodium Azide	C	4110C (2011)	$76
Specific Conductance	F	9050A	$39
Strontium	F	6010C	$10
		7000B	$26
	F and F13	6010D	$10
Sulfate	F	9035	$76
		9036	$76
		9038	$76
		9056A	$26
Sulfides	F	9030B	$76
		9031	$76
		9034	$76
		9215	$76
Thallium	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Tin	F	6010C	$10
		7000B	$26
	F and F13	6010D	$10
Titanium	F	6010C	$10
Vanadium	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
Water	F	9000	$32
		9001	$32
White Phosphorus by GC	F	7580	$116
Zinc	F	6010C	$10
		6020A	$26
		7000B	$26
		7010	$26
	F and F13	6010D	$10
		6020B	$26
4. Organics Procedures in Waste
Description	Reference	Method/s	Fee Per Method
Separatory Funnel Liquid-Liquid Extraction	F	3510C	$13
Organic Compounds in Water by Microextraction	F5	3511	$13
Continuous Liquid-Liquid Extraction	F	3520C	$13
SPE	F	3535A	$13
Soxhlet Extraction	F	3540C	$13
Automated Soxhlet Extraction	F	3541	$13
Pressurized Fluid Extraction	F	3545A	$13
Ultrasonic Extraction	F	3550C	$13
Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons	F	3560	$13
Supercritical Fluid Extraction of PAHs	F	3561	$13
SFE of PCBs and Organochlorine Pesticides	F	3562	$13
MSE	F4	3570	$13
Waste Dilution	F	3580A	$13
Waste Dilution for Volatile Organics	F	3585	$13
Alumina Cleanup	F	3610B	$13
Alumina Column Cleanup and Separation of Petroleum Wastes	F	3611B	$13
Florisil Cleanup	F	3620C	$13
Silica Gel Cleanup	F	3630C	$13
Gel-Permeation Cleanup	F	3640A	$13
Acid-Base Partition Cleanup	F	3650B	$13
Sulfur Cleanup	F	3660B	$13
Sulfuric Acid/Permanganate Cleanup	F	3665A	$13
Screening Solids for VOCs	F	3815	$76
Hexadecane Extraction and Screening for Purgeable Organics	F	3820	$76
Screening for Pentachlorophenol by Immunoassay	F	4010A	$76
Screening for 2,4-Dichlorophenoxyacetic Acid by Immunoassay	F	4015	$76
Screening for PCBs by Immunoassay	F	4020	$76
Screening for PCDDs and PCDFs by Immunoassay	F3	4025	$76
Soil Screening for Petroleum Hydrocarbons by Immunoassay	F	4030	$76
Soil Screening for PAHs by Immunoassay	F	4035	$76
Soil Screening for Toxaphene by Immunoassay	F	4040	$76
Soil Screening for Chlordane by Immunoassay	F	4041	$76
Soil Screening for DDT by Immunoassay	F	4042	$76
TNT Explosives in Soil by Immunoassay	F	4050	$76
RDX in Soil by Immunoassay	F	4051	$76
Screening Environmental Samples for Planar Organic Compounds	F	4425	$76
Triazine Herbicides by Quantitative Immunoassay	F	4670	$76
VOCs in Various Sample Matrices Using Equilibrium Headspace Analysis	F8	5021A	$13
Purge-and-Trap for Aqueous Samples	F6	5030C	$13
Volatile, Nonpurgeable, Water-Soluble Compounds by Azeotropic Distillation	F	5031	$13
VOCs by Vacuum Distillation	F	5032	$13
Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples	F2	5035A	$13
Analysis for Desorption of Sorbent Cartridges from VOST	F	5041A	$13
EDB and DBCP by Microextraction and GC	F	8011	$116
C10 – C32 Hydrocarbons	K	8015AZ 1	$116
Nonhalogenated Organics Using GC/FID	F7	8015D	$116
Aromatic and Halogenated Volatiles by GC Using Photoionization and/or Electrolytic Conductivity Detectors	F	8021B	$152
Acrylonitrile by GC	F	8031	$76
Acrylamide by GC	F	8032A	$76
Acetonitrile by GC with Nitrogen-Phosphorus Detection	F	8033	$76
Phenols by GC	F	8041A	$116
Phthalate Esters by GC/ECD	F	8061A	$116
Nitrosamines by GC	F	8070A	$116
Organochlorine Pesticides by GC	F	8081B	$152
Elemental Quantitation by GC/AED	F	8085	$116
PCBs by GC	F	8082A	$152
Nitroaromatics and Cyclic Ketones by GC	F	8091	$116
Explosives by GC	F	8095	$116
PAHs	F	8100	$116
Haloethers by GC	F	8111	$116
Chlorinated Hydrocarbons by GC: Capillary Column Technique	F	8121	$116
Aniline and Selected Derivatives by GC	F	8131	$116
Organophosphorus Compounds by GC	F	8141B	$152
Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization	F	8151A	$152
VOCs by GC/MS, including n-Hexane	F	8260B	$152
	F12 and F13	8260C/8000D	$152
VOCs by VD/GC/MS	F	8261	$152
Semivolatile Organic Compounds by GC/MS	F	8270C	$152
	F and F13	8270D/8000D	$152
Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using TE/GC/MS	F	8275A	$152
8280A: Polychlorinated Dibenzo-p-Dioxins and PCDFs by HRGC/LRMS	F	8280B	$258
PCDDs and PCDFs by HRGC/HRMS	F	8290A	$258
PAHs	F	8310	$116
Determination of Carbonyl Compounds by HPLC	F	8315A	$116
Acrylamide, Acrylonitrile, and Acrolein by HPLC	F	8316	$116
N-Methylcarbamates by HPLC	F	8318A	$116
Solvent-Extractable Nonvolatile Compounds by HPLC/TS/MS or UV Detection	F	8321B	$152
Solvent Extractable Nonvolatile Compounds by HPLC/PB/MS	F	8325	$152
Nitroaromatics and Nitramines by HPLC	F	8330A	$116
Nitroaromatics, Nitramines, and Nitrate Esters	F11	8330B	$116
Tetrazene by Reverse Phase HPLC	F	8331	$116
Nitroglycerin by HPLC	F	8332	$116
GC/FT-IR Spectrometry for Semivolatile Organics: Capillary Column	F	8410	$116
Analysis of Bis (2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR	F	8430	$116
Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry	F	8440	$116
Screening for RDX/MDX in Soil	F	8510	$76
Colorimetric Screening Method for TNT in Soil	F	8515	$76
Screening for Total VOH in Water	F	8535	$76
PCP by UV Colorimetry	F	8540	$108
TOX	F	9020B	$76
POX	F	9021	$76
TOX by Neutron Activation Analysis	F	9022	$114
EOX in Solids	F	9023	$114
TOCs	F	9060A	$76
Phenolics	F	9065	$152
		9066	$152
		9067	$152
HEM for Aqueous Samples	F	9070A	$76
HEM for Sludge, Sediment, and Solid Samples	F	9071B	$76
Screening for TRPH in Soil	F	9074	$76
Screening for PCBs in Soil	F	9078	$76
Screening for PCBs in Oil	F	9079	$76
PCBs in Waste Oil	A4.28	600/4-81-045	$152
5. Bulk Asbestos Analysis of Waste
Description	Reference	Method/s	Fee Per Method
Bulk Asbestos Analysis	A4.29	Bulk Asbestos	$228
	G	9002	$228
	G1 and A4.29	Bulk Asbestos	$228
Fiber Counting	G	7400	$228
		7402	$228
6. Radiochemistry of Waste
Description	Reference	Method/s	Fee Per Method
Alpha-Emitting Radium Isotopes	F	9315	$206
Gross Alpha and Beta	F	9310	$206
Radium-228	F	9320	$206

Historical Note

New Table 6.2.C. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.2.D. Approved Methods and Method Fees for Air and Stack Parameters

1. Ambient Air Primary and Secondary Pollutants
Description	Reference	Method/s	Fee Per Method
Carbon Monoxide	O	Appendix C	$393
Formaldehyde	F	8520	$393
Lead	O	Appendix G	$393
Nitrogen Dioxide	O	Appendix F	$393
Ozone	O	Appendix D	$393
Particulate Matter	O	Appendix B	$393
		Appendix J	$393
		Appendix L	$393
		Appendix O	$393
Sulfur Oxides	O	Appendix A	$393
2. Stationary and Stack Sources
Description	Reference	Method/s	Fee Per Method
Carbon Dioxide, Oxygen, and Excess Air	Q	Method 3C	$393
Carbon Monoxide	Q	Method 10	$393
		Method 10A	$393
		Method 10B	$393
Carbonyl Sulfide, Hydrogen Sulfide, and Carbon Disulfide	Q	Method 15	$393
Fluoride	Q	Method 13A	$393
		Method 13B	$393
		Method 14	$393
Fugitive Emissions	Q	Method 22	$393
Gaseous Organic Compounds	Q	Method 18	$393
		Method 25	$393
		Method 25A	$393
		Method 25B	$393
Hydrogen Sulfide	Q	Method 11	$393
Inorganic Lead	Q	Method 12	$393
Mercury, Total Vapor Phase	Q1	PS-12B	$393
Moisture Content	Q	Method 4	$393
Nitrogen Oxide	Q	Method 7	$393
		Method 7A	$393
		Method 7B	$393
		Method 7C	$393
		Method 7D	$393
		Method 7E	$393
		Method 20	$393
Non-methane Organic Compounds	Q	Method 25C	$393
Particulate Emissions by Asphalt Processing and Roofing	Q	Method 5A	$152
Particulate Emissions by Fiberglass Insulation Plants	Q	Method 5E	$152
Particulate Emissions of Nonsulfates	Q	Method 5F	$152
Particulate Emissions by Nonsulfuric Acid	Q	Method 5B	$152
Particulate Emissions by Pressure Filters	Q	Method 5D	$152
Particulate Emissions by Stationary Sources	Q	Method 5	$152
		Method 17	$152
Particulate Emissions by Wood Heaters	Q	Method 5G	$152
		Method 5H	$152
Petroleum Products, Heat of Combustion	I	D240-92	$76
		D240-87	$76
Petroleum Products, Hydrometer Method	I	D287-92	$76
Petroleum Products, Sulfur	I	D4294-90	$152
Sulfur and Total Reduced Sulfur	Q	Method 15A	$393
		Method 16	$393
		Method 16A	$393
		Method 16B	$393
Sulfur Dioxide	Q	Method 6	$393
		Method 6A	$393
		Method 6B	$393
		Method 6C	$393
		Method 8	$393
		Method 19	$393
		Method 20	$393
Sulfur Dioxide Removal and SO2/NO Emission Rates	Q	Method 19	$152
Sulfuric Acid Mist	Q	Method 8	$393
Vapor Tightness, Gasoline Delivery Tank	Q	Method 27	$393
Volatile Matter Density, Solids and Water from Surface Coatings	Q	Method 24	$393
		Method 24A	$393
Volatile Matter and Density of Printing Inks	Q	Method 24A	$393
VOCs	Q	Method 21	$393
	S1	TO-3	$152
		TO-14A	$152
		TO-15	$152
VOCs in Vapor	F1	8260B AZ (Vapor) (0.0)	$152
Wood Heaters, Certification and Burn Rates	Q	Method 28	$393
		Method 28A	$393
3. ADEQ Emission Test
Description	Reference	Method/s	Fee Per Method
Particulate Emissions in the Presence of Sulfuric Acid Mist/Sulfur Oxides	R	Method A1	$393
4. National Emission Standards for Hazardous Air Pollutants
Description	Reference	Method/s	Fee Per Method
Arsenic	S	Method 108	$393
		Method 108A	$393
		Method 108B	$393
		Method 108C	$393
Beryllium	S	Method 103	$393
		Method 104	$393
Mercury	S	Method 101	$393
		Method 101A	$393
		Method 102	$393
		Method 105	$393
Polonium 210	S	Method 111	$393
Vinyl Chloride	S	Method 106	$393
		Method 107	$393
		Method 107A	$393
5. Determination of Metals in Ambient Particulate Matter
Description	Reference	Method/s	Fee Per Method
Digestion of Ambient Matter	O3	IO-3.1	$7
Aluminum	O1	IO-3.4	$10
	O2	IO-3.5	$26
Antimony	O1	IO-3.4	$10
	O2	IO-3.5	$26
Arsenic	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Barium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Beryllium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Bismuth	O1	IO-3.4	$10
Cadmium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Calcium	O1	IO-3.4	$10
Cesium	O1	IO-3.4	$10
Chromium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Cobalt	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Copper	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Germanium	O1	IO-3.4	$10
Gold	O1	IO-3.4	$10
Indium	O1	IO-3.4	$10
Iron	O1	IO-3.4	$10
Lanthanum	O1	IO-3.4	$10
Lead	O1	IO-3.4	$10
	O2	IO-3.5	$26
	O4	EQL-0510-191	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Lithium	O1	IO-3.4	$10
Magnesium	O1	IO-3.4	$10
Manganese	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Mercury	O1	IO-3.4	$10
	Q	Method 29 – CVAA	$52
Molybdenum	O1	IO-3.4	$10
	O2	IO-3.5	$26
Nickel	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Niobium	O1	IO-3.4	$10
Palladium	O1	IO-3.4	$10
Phosphorus	O1	IO-3.4	$10
	Q	Method 29 – ICP	$10
Platinum	O1	IO-3.4	$10
Potassium	O1	IO-3.4	$10
Rhenium	O1	IO-3.4	$10
Rhodium	O1	IO-3.4	$10
Ruthenium	O1	IO-3.4	$10
Samarium	O1	IO-3.4	$10
Selenium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Silicon	O1	IO-3.4	$10
Silver	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Sodium	O1	IO-3.4	$10
Strontium	O1	IO-3.4	$10
Tantalum	O1	IO-3.4	$10
Tellurium	O1	IO-3.4	$10
Thallium	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Thorium	O2	IO-3.5	$26
Tin	O1	IO-3.4	$10
Titanium	O1	IO-3.4	$10
Tungsten	O1	IO-3.4	$10
Uranium	O2	IO-3.5	$26
Vanadium	O1	IO-3.4	$10
	O2	IO-3.5	$26
Ytrrium	O1	IO-3.4	$10
Zinc	O1	IO-3.4	$10
	O2	IO-3.5	$26
	Q	Method 29 – ICP	$10
		Method 29 – ICPMS	$26
Zirconium	O1	IO-3.4	$10

Historical Note

New Table 6.2.D. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.2.E. Methods Director-Approved under R9-14-610(E) and Method Fees

Description	Reference	Method/s	Fee Per Method
Chromatographic Method	-	Any	$116
Mass Spectrometric Method	-	Any	$152
Toxicity Method	-	Any	$194
Other Method	-	Any	$75

Historical Note

New Table 6.2.E. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.3. Instrumentation Fees

Description	Subtype, if any	Fee Per Instrument
Atomic Absorption	Cold Vapor	$76
	Flame Burner	$76
	Graphite Furnace	$76
	Hydride Generator	$76
	Other	$76
Counters for Radioactivity	-	$76
Gas Chromatograph	Electron Capture	$76
	Flame Ionization	$76
	Flame Photometric	$76
	Halide Specific	$76
	Nitrogen/Phosphorus	$76
	Photoionization	$76
	Other	$76
Gas Chromatograph/Mass Spectrometer	High Resolution	$194
	Other than High Resolution	$152
High Pressure Liquid Chromatograph	Ultraviolet	$76
	Fluorescence	$76
	Other	$76
High Pressure Liquid Chromatograph/Mass Spectrometer	-	$152
Inductively Coupled Plasma	-	$76
Inductively Coupled Plasma/Mass Spectrometer	-	$152
Ion Chromatograph	-	$76
Automated Autoanalyzer	-	$76
Mercury Analyzer	-	$76
Organic Halide, Total	-	$76
Transmission Electron Microscope	-	$396
X-Ray Diffraction Unit	-	$76

Historical Note

New Table 6.3. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Table 6.4. Alternate Default Limits

QUALITY CONTROL PARAMETERS WITHOUT ACCEPTANCE CRITERIA SPECIFIED IN THE METHOD	DEFAULT LIMITS
Matrix Spike/LFM (processed or non-processed)	LCS/LFB
Matrix Spike/LCS for 8000 methods	±30%.
LCS/LFB (processed or non-processed)/Second source reference standard	CCV/continuing IPC
LOQ/MRL (non-processed)	CCV/continuing IPC or ± 50%
LOQ/MRL (processed)	LCS/LFB or ± 50%
Methods that do not specify the LOQ/MRL	± 50%
QCS (non-processed)	ICV/continuing IPC/manufacturer’s limits
QCS (processed)	LCS/LFB/manufacturer’s limits
IDOC limits	LFB/LCS
LFB/LCS/LFM/duplicate RPD	IDOC limits/20%
Non-CCC compounds	CCC limits
ICV/CCV	± 10%
500, 600, 1600, and 8000 series methods that do not specify surrogates or acceptance limits for surrogates	70-130%.
500, 600, 1600, and 8000 series methods that do not specify internal standards or acceptance limits for internal standards	70-130%.
Methods that do not list a precision measurement	20% RPD

Historical Note

New Table 6.4. made by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).

Historical Note

New Section adopted by final rulemaking at 7 A.A.R. 184, effective December 15, 2000 (Supp. 00-4). Section R9-14-621 renumbered from R9-14-620 and amended by final rulemaking at 12 A.A.R. 4798, effective December 5, 2006 (Supp. 06-4). Amended by final rulemaking at 22 A.A.R. 2683, effective October 1, 2016 (Supp. 16-3).